浙南特色中草药菜头肾的质量标准研究

打开文本图片集
【中图分类号】R284.1 【文献标志码】A 【文章编号】1007-8517(2025)16-0027-07
DOI: 10.3969/j .issn.1007-8517.2025.16. zgmzmjyyzz202516007
StudyontheQualityStandardforRootofStrobilanthesSarcorrhizus aCharacteristicChineseHerbalMedicinein ZhejiangSouthern
CUI Xiurong1LI Jianqiang²LU Lun³WANG Hong²ZHANG Liping1ZHU Yindi2* 1. Wenzhou Institute for Food and Drug Control,Wenzhou 325038,China;
2.School of Chinese Medicine,Wenzhou Medical University,Wenzhou 325035,China; 3.Anhui Institute ofQuality and Standardization,Hefei 23Oo51,China
Abstract:ObjectiveTostudyand improvethequality standardfor Strobilanthessarcorhizus.Methods Theappearanceand characteristics of S .sarcorhizus were described. Qualitative identification of S.sarcorrhizus was performed using microscopic identification.Thin-layerchromatogaphy(TC)wasperformedforidentificationwithtereferencesubstanceofforsythiasideBasthontrol. AccordingtotegeneralprinciplsofteChineseParmacopoeia(22edition,Vol.4),thewaterconent,totalash,acidsoluble ash and water-soluble extract of S .sarcorrhizuswere determined. Thecontent determinationmethod for S .sarcorrhizuswas establishedusinghigh-performanceliquidchromatogaphy(HPLC),withforsythiasideBasthequalitycontrolindex.Thecontentofpolysaccharide wasdetermined byphenol-sulfuricacid method using D-glucose asreference substance.Results Thestructureof the fleshy roots of S ,sarcorrhizus belongs toafew cases of dicotyledonous roots,with large pith.Thepowder microscopic characteristics havethecharacteristicsofjasmineplants.TC methodwasspecificandsimple.Thewatercontent,totalash,acid-insolubleash, water-solubleextractive,thecontentofforsythiasideBandthecontentofpolysaccharideofallsamplesvariedintherangesof10. 4% (204号 -12.6 , 3.9%-4.9% , 0.05%-0.49% , 67.1%-81.0% , 0.11%-1.29% and 24.45%-52.67% ,respectively,the methodologicalinvestigationofcontentdeterminationmeetsterequirements.ConclusionTheestablishedmethodcanbeusedforquality control of S sarcorrhizus. The preliminary quality standard of S :sarcorrhizus are as follows:the water content should not be higher than 14. 0% ,thetotalash should not behigher than 6.0% ,the water-soluble extract should not be lower than 60.0% ,the contentof forsythiasideB should not be lower than 0.37% ,and the content of polysaccharide should not be lower than 24.0% calculated 基金项目:温州市科技项目(Y20190197,N20210002);温州市科协项目(2019KXCX-KT)。(剩余10166字)