衍生化气相色谱内标法测定精制苏子油中脂肪酸成分含量

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开放科学（资源服务）标识码（OSID）：

AGCMethodCombedwithDerivatzationandInternalStandardfortheDeterminatonoftheFattcidsinRefinedPerilaSeed Oil

HAO Jian-xin1，²，HUANG Yu-yao1，LU Liα et al（1. Guangzhou Heyi Medical Technology Co.，Ltd.，Guangzhou，Guangdong 510970; Sichuan Haoyun Pharmaceutical Co.，Ltd.，Guangyuan，Sichuan 628017）

AbstractObjective]ToestablishaGCmetodcombinedwithdrivatiationandtealstandardforthedeteminationoffatyacidsinr finedperllasdilMetdTidpillseedilsaplewaspreparedyethsterifationwiheptadeaicacidsite nalstandard，andnalydygilentcapilarycolunDB-waouledwithameiozatodetetorFD）．Resultelineaelatip of palmitic acid，steraric acid，oleic acid，linoleic acid and ∝ -linolenic acidwas good（ R2⩾0 .9990）within the range of O.O31 92- 0.319 20，0.010 68-0.106 80，0.078 40-0.78400，0.0768-0.768 00 and 0.30000-3.000000mg/mL ，respectively. The precisions and recoveries were up to the mustard，and the contents of the fatty acids were 5. 98% ， 1.87% ， 15. 1% ， 14.6% and 53.9% ，respectively. [Conclusion]Tismetodwasuratefothedeterinationoffivetycidsinefidperillseedoilandwouldbeusedasafective method for quality control and function evaluation of perilla seed oil.

KeyWordsPerilla seed oil;Fatty acid;Content;GC;Internal standard;Derivatization

紫苏[Perilla frutescens（L.）Britt.]，古名荏，又名引子、白苏、苏子、苏草、苏麻、香苏、桂荏等，属于唇形科紫苏属的一年生草本植物[1]。（剩余6178字）