萃取法测定地表水中挥发酚的监测分析要点研究

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文章编号：1674-6139（2025）05-0135-04

中图分类号：X832文献标志码：B

KeyPoints for Monitoring and Analysis of Volatile Phenols in Surface Water using Extraction Method

WangJialong1，LiuRui1，MaYukun²

（1.Microbiology Research Institute，Heilongjiang Academy of Sciences，Harbin 150010，China; 2.HeilongjiangProvincial Environmental MonitoringCenter，Harbin15oo9O，China）

Abstract：ThisarticleliststhemainanalyticalmethodsnddetectionlimitsfordeterminingvolatilephenolsathomeandabroadAt present，the4aminoantipineextractionspectrophotometricmetodisteainmtodfodetermigvolatilepenolsinsufacete whichisaclasicmethod.Thismethodhashghsensitivitygodprecisionandacuracy，buttherearealsomanyinfluencingfactors. Thisarticleconductsanin-depthanalysisofthinfuencingfactorsofthedeterminationofvolatilephenolsinsurfacewaterItstudies anddiscussesfromaspectssuchasreagentsandtheirpuriy，interferenceeffects，therderofreagentadition，theinfluenceof pH on colordevelopmentesults，ndthechangesofsmplesovertime.Itprovidesotherprecautiostatecttheeterinationresultsiex periments and the purification method of 4- aminoantipyrine reagent.This ensures the smooth process of the 4-aminoantipyrine extraction spectrophotometric experiment and guarantees the accuracy of the monitoring results.

Key words：4-aminoantipyrine；volatile phenols；extraction；influencing factors；interfering substances

前言

根据酚类是否能随水蒸气蒸馏而出分为挥发酚和不挥发酚，沸点在 230% 以下随水蒸气蒸馏出的为挥发酚[1]。（剩余3371字）